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Beilstein J. Org. Chem. 2014, 10, 2531–2538, doi:10.3762/bjoc.10.264
Graphical Abstract
Scheme 1: Synthesis of Nortricyclenes from Norbornenes.
Figure 1: X-ray crystal structure of 5a with 30% thermal ellipsoids.
Scheme 2: KO2-mediated synthesis of tetrachloro-substituted 3-methylenenortricyclenes. Reaction conditions: A...
Scheme 3: Mechanism investigations.
Scheme 4: Plausible mechanism of the KO2-mediated reaction.
Figure 2: X-ray crystal structure of 8a with 30% thermal ellipsoids.
Scheme 5: Plausible mechanism of the acylation reaction of 3-methylenenortricyclenes.